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Beilstein J. Org. Chem. 2013, 9, 951–959, doi:10.3762/bjoc.9.109
Graphical Abstract
Figure 1: Schematic representation of the 3D-printed reactionware devices employed in this work showing the i...
Figure 2: Flow system setup, where a R1 is connected to the syringe pumps and the ATR-IR flow cell with stand...
Figure 3: Carbonyl compounds and primary amines used in the syntheses reported in this work. Carbonyl compoun...
Figure 4: ATR-IR spectra of the synthesis of compounds 3b (on the left) and 3d (on the right). The spectrum o...
Figure 5: (a) IR spectra of benzaldehyde at different concentrations. The solvent peak at 1022 cm−1 remains c...
Figure 6: Comparison of the IR spectra of imine 3a, derived from benzaldehyde (1a) and aniline (2a), synthesi...
Figure 7: Representation of the setup for the two-step flow reaction employed in this work. The first reactor...
Figure 8: Example of an ATR-IR graph in which an imine spectrum is compared with the reduced imine spectrum.